Nitric Acid, ASTM A, Practice C, (Huey Test) The specimens are boiled for five periods, each of 48 hours, in a 65 per cent solution of nitric acid. The corrosion. employed to measure the relative susceptibility of austenitic stainless steels to intergranular attack. ASTM A Practice C, boiling nitric acid test is also known . Ferric Sulfate – Sulfuric Acid, ASTM A – Practice B (Stretcher Test). Ferric Sulfate Nitric Acid, ASTM A, Practice C, (Huey Test). Nitric Acid, ASTM A
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The chart below comes from the ASTM A standard pratice selection of the appropriate test by alloy type:. Based on your materials, application, and requirements, the other 4 methods provide specific focuses. For example, in highly oxidizing solutions, intergranular attack can occur due to intermetallic phases, while attack of carbides may occur somewhat less oxidizing solutions.
ASTM A Testing: An Overview of Intergranular Corrosion | Element
We provide intergranular corrosion evaluation, salt spray testing, stress corrosion, and various other methods to simulate exposure of your products or materials to corrosive environments. Practice E, the Strauss test, is performed to assess attack associated with chromium-rich carbide formation; it does not detect susceptibility to sigma phase formation.
Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility.
ASTM A is a common intergranular corrosion testing method that can quickly screen batches of material to determine corrosion susceptibility. What is your typical turnaround time? A different ASTM A test method must be used to quantify the level of corrosion or to disqualify a material for use. These practices include five intergranular corrosion tests, namely: Discover perspectives, resources, and advice from our world-leading Engaged Experts.
Choosing the correct method s rely on a complete understanding of your material and processes, as well as praactice concept of corrosion itself.
Link to Active This link will always route to the current Active version of the standard. Referenced Documents purchase separately The documents listed below are referenced within the subject standard but are not provided as part of the standard.
The Oxalic Acid test is also only applicable to corrosion associated with chromium carbide precipitates and is only useful for specific material grades. It is informational only and not an official part of the standard; the full text of the standard itself must be referred to for its use and application. The weight loss is calculated after each step, and reveals if the sample has been properly heat-treated.
Metals like stainless steels and aluminum contain elements such as niobium and chromium, often integrated because of their natural corrosion resistance. Due to the variance of attack in different materials, numerous methods Practices B-F are used to assess intergranular corrosion.
Each ASTM A Practice specification includes a list of the grades of stainless steels and the acceptable etch structures for the specific alloys. The inch-pound equivalents are in parentheses and may be approximate. The test uses a visual inspection of the surface of the bent specimen to determine pass or fail. ASTM A testing is a popular method of choice due to the variety of practices available and the relatively short turnaround for results.
Sensitization causes the grain boundaries of wstm material pratice precipitate, creating carbide deposits and causing the material to be susceptible to intergranular attack. The test is generally performed for acceptance of materials, but not sufficient for rejection of materials.
Historical Version s – view previous versions of standard. Our knowledgeable scientists have the experience and expertise necessary to determine the most appropriate intergranular attack testing methods for your material while providing actionable results you can rely on. Please specify the maximum allowable corrosion rate and any available data on the sensitizing heat treatment performed.
Intergranular corrosion occurs as a result of precipitation of nitridescarbidesand other intermetallic phasessuch as sigma phase, that occurs along the grain boundaries. Practice A, the oxalic acid etch test is used as a rapid technique to screen samples of certain stainless steel grades to ensure they are not susceptible to intergranular attack sensitization.
This method is preferable for chromium depletions and corrosion in intermetallic phases. To understand intergranular corrosion testing or intergranular attack commonly abbreviated as IGC or IGAit is important to understand what causes the process to occur.
The Oxalic Acid test is only used to ensure that no corrosion exists; samples are labeled either “Acceptable” or “Suspect”.
From macroscopic imaging to Scanning Electron Microscopy, Element provides turnkey metallographic services using state-of-the-art equipment. A26 oxalic acid test is commonly used before the Strauss test to determine if a sample is susceptible; samples that pass method A will generally show low corrosion rates in the Strauss test. In many cases we can reduce that to as little as 24 hours more than the required testing time if you need fast results.
ASTM does not give any warranty express or implied or make any representation that the contents of this abstract are accurate, complete or up to practjce.
It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Strauss test specimens are boiled in q262 Copper Sulfate – Sulfuric Acid mixture for 15 hours. Contact us now for pricing or a quote! These tests are often run as a qualification test to ensure each batch of stainless steel is properly prepared.
Please share this page: A bend test followed by a visual or micro-examination are used to determine “Pass” or “Fail” of test specimens. However, when a material is exposed to high temperatures for long periods of time, a process called sensitization may occur. Awtm Item s – proposed revisions of this standard.
A recent publication on intergranular corrosion. How do you select the right ASTM corrosion testing method for your material?